| Week of | Laboratory Experiment / Exercise | Pages |
|---|---|---|
| Jan. 24 | Introduction, Check-in, Lab Safety, Citing Information in the Laboratory | Technique
1 Manual pp. 1-13 |
| Jan. 31 | Physical Properties Melting Point Refractive Index | Techniques 1;
3.9; 24; 9 (9.1-9.5, 9.7-9.9) Manual pp. 17-22 |
| Feb. 7 | Recrystallization Vacuum Filtration | Techniques 11 (11.1-11.3A, C-D, 11.5,
11.6, 11.8-11.10); 6 (6.2, 6.5, 6.6, 6.9) Manual pp. 23-26 |
| Feb. 14 | Lecture - IR,
MS, UV Spectroscopy Spectroscopy of Unknown Spectroscopy Problem Set | Techniques 25
(25.9-25.14); 28 Solomons & Fryle Sec. 2.16; 9.13-9.17; 13.9 Manual pp. 27-38 |
| Feb. 21 | ID of an Unknown
(IR continued) Simple Distillation to Determine Boiling Point | Techniques 3 (3.3-3.8); 13.1; 14 (14.1-14.3); 25 (25.1, 25.2, 25.4, 25.7) |
| Feb. 28 | Gas Chromatography: Acetates | Technique 22 (22.1-22.7, 22.9, 22.10,
22.12) Manual pp. 39-41 |
| Mar. 7 | Simple and Fractional Distillation | Technique 15.1-15.6 Manual pp. 43-46 |
| Mar. 14 | Spring Break | None |
| Mar. 21 | Gas Chromatography: Distillate | Technique 22 (22.8, 22.11, 22.13,
22.14) Manual p. 47 |
| Mar. 28 | Synthesis of tert-BuCl | Technique 12 (12.1-12.4,
12.8-12.10) Experiment 21: pp. 172-174 Manual pp. 49-50 |
| Apr. 4 | Synthesis of Cyclohexene | Solomons & Fryle
pp. 297-302 Experiment: pp. 179-183 Manual pp. 51-52 |
| Apr. 11 | Qualitative Organic Analysis: alkanes, alkenes, alkynes, aromatics, alkyl & aryl halides, alcohols | Experiment 55: pp. 446-461,
464-468, 483-487 Manual pp. 53-57 |
| Apr. 18 | Qualitative Organic Analysis, continued | None |
| Apr. 25 | Reserved for make-up class, if necessary | TBA |
| May 2 | Final Exam (Cumulative) and Check-out | None |